ML-PHILMUS-001
Jan 17 05:45pm - Jan 17 09:45pm

Jim Rocca for B J Philmus, Dept of Pharmaceutical Sciences, Oregon State University, Corvallis. Sample from June of 2019: About 400-ug sample with 10% 2H-labeling. Largish vial required 0.55-ml of CHCl3. Recovered dry from 5-mm tube and taken up in 35-ul of CDCl3. 1H and long 13C. Not much signal, and possible contamination from the amylenes in the previous CHCl3 solution.